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Stability and Activity of Zn/MCM-41 Materials in Toluene Alkylation: Microwave Irradiation vs Continuous Flow
dc.contributor.author | Carraro, Paola M. | |
dc.contributor.author | Goldani, Bruna S. | |
dc.contributor.author | Alves, Diego | |
dc.contributor.author | Sathicq, Ángel | |
dc.contributor.author | Eimer, Griselda A. | |
dc.contributor.author | Romanelli, Gustavo P. | |
dc.contributor.author | Luque, Rafael | |
dc.date.accessioned | 2019-02-25T11:51:38Z | |
dc.date.available | 2019-02-25T11:51:38Z | |
dc.date.issued | 2019 | |
dc.identifier.uri | http://hdl.handle.net/10396/17947 | |
dc.description.abstract | Zn/MCM-41 mesoporous materials have been prepared via classic wet impregnation, employing zinc nitrate as precursor and tested for activity and stability in the Friedel-Crafts alkylation of toluene with benzyl chloride under microwave irradiation and continuous flow. The modified materials were characterized by means of a number of analytical techniques, and surface and textural properties were thoroughly checked. Materials containing the highest Zn loading (15 wt %) provided full conversion after 5 min reaction under microwave irradiation (300 W, 120 _C). Materials were proved to be stable and reusable for several cycles with an optimum performance under continuous flow conditions. | es_ES |
dc.format.mimetype | application/pdf | es_ES |
dc.language.iso | eng | es_ES |
dc.publisher | MDPI | es_ES |
dc.rights | https://creativecommons.org/licenses/by/4.0/ | es_ES |
dc.source | Catalysts 9(2), 136 (2019) | es_ES |
dc.subject | MCM-41 | es_ES |
dc.subject | Friedel–Crafts alkylation | es_ES |
dc.subject | Microwave | es_ES |
dc.subject | Continuous flow | es_ES |
dc.subject | Zinc | es_ES |
dc.title | Stability and Activity of Zn/MCM-41 Materials in Toluene Alkylation: Microwave Irradiation vs Continuous Flow | es_ES |
dc.type | info:eu-repo/semantics/article | es_ES |
dc.relation.publisherversion | http://dx.doi.org/10.3390/catal9020136 | es_ES |
dc.rights.accessRights | info:eu-repo/semantics/openAccess | es_ES |