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One-Pot Cu/TiO2 Nanoparticles Synthesis for Trans-Ferulic Acid Conversion into Vanillin
dc.contributor.author | Gómez-López, Paulette | |
dc.contributor.author | Lázaro, Noelia | |
dc.contributor.author | Alvarado-Beltrán, Clemente G. | |
dc.contributor.author | Pineda, A. | |
dc.contributor.author | Balu, Alina M. | |
dc.contributor.author | Luque, Rafael | |
dc.date.accessioned | 2019-11-04T12:24:44Z | |
dc.date.available | 2019-11-04T12:24:44Z | |
dc.date.issued | 2019 | |
dc.identifier.uri | http://hdl.handle.net/10396/19057 | |
dc.description.abstract | In this study, the co-synthesis of TiO2 and Cu metallic nanoparticles obtained via one-pot cost-efficient hydrothermal process has been addressed. Different nanocatalysts with Cu contents were characterized by X-ray diffraction, nitrogen porosimetry, scanning electron microscopy, and transmission electron microscopy. The TiO2 and Cu metallic nanoparticles were synthesized with copper loading up to one (Cu/Ti atomic ratio). Synthesized catalysts exhibited pore sizes in the mesoporous range and high surface areas above 150 m2/g. The particle size for TiO2 presented a homogeneous distribution of approximately 8 nm, moreover, Cu nanoparticles varied from 12 to >100 nm depending on the metal loading. The nanostructured materials were successfully tested in the conversion of trans-ferulic acid into vanillin under sustainable conditions, achieving the best performance for 0.3 Cu/Ti atomic ratio (70% vanillin yield). | es_ES |
dc.format.mimetype | application/pdf | es_ES |
dc.language.iso | eng | es_ES |
dc.publisher | MDPI | es_ES |
dc.rights | https://creativecommons.org/licenses/by/4.0/ | es_ES |
dc.source | Molecules 24(21), 3985 (2019) | es_ES |
dc.subject | One-pot synthesis | es_ES |
dc.subject | TiO2 | es_ES |
dc.subject | Cu nanoparticles | es_ES |
dc.subject | Vanillin | es_ES |
dc.subject | Trans-ferulic acid | es_ES |
dc.subject | Heterogeneous catalysis | es_ES |
dc.title | One-Pot Cu/TiO2 Nanoparticles Synthesis for Trans-Ferulic Acid Conversion into Vanillin | es_ES |
dc.type | info:eu-repo/semantics/article | es_ES |
dc.relation.publisherversion | http://dx.doi.org/10.3390/molecules24213985 | es_ES |
dc.relation.projectID | Gobierno de España. CTQ2016-78289-P | es_ES |
dc.rights.accessRights | info:eu-repo/semantics/openAccess | es_ES |